Circle Chart for the Monitoring of Maxima in Periodic Processes

An important process characteristic is process maxima as it is often an important quality or performance parameter. Such measurements often play a vital role in process analysis and have to be monitored carefully. In this paper, we consider the problem of monitoring process maxima when the process exhibits a kind of periodicity. A circle chart for periodical process maxima with or without seasonal patterns monitoring is developed and studied, by modeling the process maxima using the extreme value distribution. Mean normalization is applied for periodic process monitoring with seasonal patterns to facilitate comparison between different sections and periods. The average cycle run length is proposed to measure charting efficiency. Copyright © 2014 John Wiley & Sons, Ltd.     

Visualization Approaches for Evaluating Ridge Regression Estimators in Mixture and Mixture‐Process Experiments

When the component proportions in mixture experiments are restricted by lower and upper bounds, the input space of a designed experiment space can become an irregular region that can induce multicollinearity problems when estimating the component proportion parameters. Thus, ridge regression provides a beneficial means of stabilizing the coefficient estimates in the fitted model. Previous research has focused on using prediction variance as a metric for determining an appropriate value of the ridge constant, k. We use visualization techniques to illustrate and evaluate ridge regression estimators and the robustness of estimation with respect to the variance and the bias. The addition of bias allows better balancing between the stability of the estimators and minimally changing the estimates. We illustrate the graphical methods with mixture and mixture‐process examples from the literature. Copyright © 2014 John Wiley & Sons, Ltd.     

Monitoring Highly Correlated Multivariate Processes Using Hotelling's T2 Statistic: Problems and Possible Solutions

Hotelling's T² statistic is the default control statistic for continuous multivariate data, but there are dangers in applying this statistic without the appropriate level of checks and balances. This paper discusses the potential issues with using the Hotelling's T² statistic when the quality variable measures are highly correlated and provides some solutions that will help mitigate the risks with applying the Hotelling's T² control charts in such practical examples. Copyright © 2014 John Wiley & Sons, Ltd.     

VIMP中结构拐角对纤维预成型体渗透特性的影响

采用真空导入模塑工艺(VIMP)制备纤维增强聚合物基复合材料多墙结构件时,多墙体拐角处的纤维弯曲变形可能导致多墙体局部渗透特性发生变化。通过可视化流动实验考察了拐角对多墙体渗透特性和树脂流动行为的影响。结果表明:无论是否使用导流介质,多墙体中的拐角对树脂流体在VIMP灌注过程中都具有局部阻力作用,降低了树脂充模流动速度和多墙体整体表观渗透率,即存在拐角效应;拐角处铺放导流介质能有效降低拐角效应;随着拐角到注胶口的距离增大,整体表观渗透率表现为先下降后上升。     

基于LSSVM的真空玻璃传热过程建模

真空玻璃传热过程隔热性能和质量评价关键指标-传热系数(U值)受真空度影响,难以精确检测。为实现真空玻璃隔热性能和质量的快速评定,建立了基于LSSVM的真空玻璃传热过程智能模型,应用MATLAB软件和实验数据,对真空玻璃传热过程进行了模拟,在线预测了真空玻璃传热后侧(非热源侧)的中心温度。结果表明:模型理论正确,预测迅速(时间1 s),误差小(相对误差1.2%),为真空玻璃隔热性能和真空玻璃质量的快速评定提供了一种新的技术手段。同时,也为后续研究能将温度参数预测转化为传热系数预测奠定一定的理论和应用基础。     

CRGP柔性导电薄膜及其超级电容器制备与性能

以CNFs膜为基材,采用层层自组装法制备CNFs/RGOn膜,通过原位聚合法在膜表面聚合PANI,制备复合导电CRGP膜电极并组成超级电容器S-RGP。研究采用UV-vis光谱、XRD、SEM等对CRGP膜的吸光度、结晶特性与形态进行测试表征,同时系统测试了S-RGPCV曲线、GCD、EIS等电化学性能。结果表明:原位聚合法得到CRGP膜表面不均匀,PANI层与基材间存在间隙,存有活性物质,导致S-RGP内阻较小;S-RGP的ESR低、柔性良好;由于原位聚合的PANI层较厚,电容器S-RGP具有一定的电致变色特征。     

60Si2MnA钢片弹簧断裂失效分析

某60Si2MnA钢片弹簧在使用10h后出现批量断裂,对断裂片弹簧进行了化学成分分析、硬度测试、金相检验以及断口微观形貌观察,以查明其断裂原因。结果表明:片弹簧断裂是由于在酸洗、电镀过程中析氢反应的发生,使其产生氢脆现象;同时由于热处理工艺过程控制不当,造成组织异常,硬度高于技术要求,加快了其氢脆倾向,最终导致片弹簧在外应力作用下发生氢脆断裂。     

单晶多孔ZnO制备及对室内空气污染物的气敏性能的研究

通过使用对液相法合成的前驱体进行煅烧的方法成功的制备了具有单晶多孔结构的Zn O纳米片。通过X射线衍射仪(XRD)、环境扫描电子显微镜(FESEM)、高分辨透射电子显微镜(TEM)对单晶多孔Zn O纳米片进行了结构以及形貌的表征和分析。以其为敏感膜,制作气体传感器,对室内空气污染物,包括苯和甲醛,进行检测。结果显示单晶多孔Zn O纳米片对苯和甲醛都有着良好的响应,且响应和恢复时间都非常迅速。对敏感机理以及材料的结构对响应时间的影响也进行了较深入的探讨。     

非晶态Ni-Fe-P合金屏蔽织物的工艺优化及耐蚀性研究

通过在已化学镀铜涤纶织物上电沉积非晶态Ni-Fe-P合金,制备出一种镀层致密均匀的柔性金属化屏蔽织物。研究和分析了电流密度、温度和p H值对合金织物方阻值、增重率及屏蔽效能的影响,从而制定出最佳工艺。通过对比腐蚀前后非晶态Ni-Fe-P合金和非晶态Ni-P合金镀层表面形貌、成分和电磁屏蔽效能可以得出,在电流密度为8.7 A/dm2,温度为60℃,p H值=1.5的工艺条件下所制备的非晶态NiFe-P合金织物结晶更加细化、光亮,致密性和均质性都得以明显提高,并具有良好的耐腐蚀性能,且在300 k Hz~1.5 GHz频率范围内的电磁屏蔽效能达到了69.20~80.30 d B。     

基于AHP-Fuzzy法的水下爆破设计方案优选

针对水下爆破设计参数的多样性及影响因素的复杂性,结合层次分析法(AHP)和模糊数学(Fuzzy)综合评价方法,建立水下爆破设计方案优选模型。权重计算可以反映各个准则及指标对目标的影响程度,为克服权重赋值过程的主观性,该模型采用判断矩阵对权值进行分配。将该模型运用于嘉陵江航道整治三期工程的爆破设计优选,经计算方案1#为最优方案。采用方案1#进行爆破施工,爆区临近桥梁的振速得到很好的控制,岩碴块度达到要求,清碴效果良好。